578-57-4

  • Product Name:2-Bromoanisole
  • Molecular Formula:C7H7BrO
  • Purity:99%
  • Molecular Weight:187.036
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Product Details;

CasNo: 578-57-4

Molecular Formula: C7H7BrO

Appearance: colourless liquid

factory and supplier 578-57-4 2-Bromoanisole in stock

  • Molecular Formula:C7H7BrO
  • Molecular Weight:187.036
  • Appearance/Colour:colourless liquid 
  • Vapor Pressure:0.21mmHg at 25°C 
  • Melting Point:2 °C(lit.) 
  • Refractive Index:n20/D 1.573(lit.)  
  • Boiling Point:215.999 °C at 760 mmHg 
  • Flash Point:96.667 °C 
  • PSA:9.23000 
  • Density:1.443 g/cm3 
  • LogP:2.45770 

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578-57-4 Process route

2-hydroxybromobenzene
95-56-7

2-hydroxybromobenzene

methyl iodide
74-88-4

methyl iodide

2-bromoanisole
578-57-4

2-bromoanisole

Conditions
Conditions Yield
2-hydroxybromobenzene; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1.16667h; Inert atmosphere;
methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 19h; Inert atmosphere; Reflux;
97%
With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h; Inert atmosphere;
96%
With potassium carbonate; In acetonitrile; at 81 ℃; for 4h; Inert atmosphere;
95%
With potassium hydroxide; In CD2Cl2; hexane; acetonitrile;
89%
With sodium hydroxide; In diethyl ether; ethanol;
With potassium hydroxide; In ethanol; toluene;
With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
2-Methoxyphenylboronic acid
5720-06-9

2-Methoxyphenylboronic acid

2-bromoanisole
578-57-4

2-bromoanisole

Conditions
Conditions Yield
With N-Bromosuccinimide; In acetonitrile; at 80 ℃; for 12h;
97%
With tetrabutylammomium bromide; copper(ll) bromide; In water; at 100 ℃; for 8h; Sealed tube;
82%
With 1,10-Phenanthroline; oxygen; potassium bromide; copper(ll) bromide; In N,N-dimethyl-formamide; at 130 ℃; for 20h;
67%
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sodium methylate; In methanol; water; acetonitrile; at 23 ℃;
94 % Chromat.

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