6372-42-5
- Product Name：Cyclohexyldiphenylphosphine
- Molecular Formula：C18H21 P
- Purity：99%
- Molecular Weight：268.338
Product Details;
CasNo： 6372-42-5
Molecular Formula： C18H21 P
Appearance： white to light yellow crystal powder
factory and supplier 6372-42-5 Cyclohexyldiphenylphosphine in stock
- Molecular Formula:C18H21 P
- Molecular Weight:268.338
- Appearance/Colour:white to light yellow crystal powder
- Vapor Pressure:1.85E-05mmHg at 25°C
- Melting Point:58-62 ºC
- Boiling Point:374 °C at 760 mmHg
- Flash Point:189.4 °C
- PSA：13.59000
- LogP:4.45200
Cyclohexyldiphenylphosphine(Cas 6372-42-5) Usage
InChI:InChI=1/C18H21P/c1-4-10-16(11-5-1)19(17-12-6-2-7-13-17)18-14-8-3-9-15-18/h1-2,4-7,10-13,18H,3,8-9,14-15H2
6372-42-5 Relevant articles
Synthesis method of phosphine (III) compound
-
Paragraph 0020, (2021/11/27)
The invention aims to provide an aryl ph...
A Lewis Base Nucleofugality Parameter, NFB, and Its Application in an Analysis of MIDA-Boronate Hydrolysis Kinetics
García-Domínguez, Andrés,Gonzalez, Jorge A.,Leach, Andrew G.,Lloyd-Jones, Guy C.,Nichol, Gary S.,Taylor, Nicholas P.
supporting information, (2022/01/04)
The kinetics of quinuclidine displacemen...
Direct and Scalable Electroreduction of Triphenylphosphine Oxide to Triphenylphosphine
Manabe, Shuhei,Sevov, Christo S.,Wong, Curt M.
, p. 3024 - 3031 (2020/03/10)
The direct and scalable electroreduction...
Versatile Visible-Light-Driven Synthesis of Asymmetrical Phosphines and Phosphonium Salts
Arockiam, Percia Beatrice,Lennert, Ulrich,Graf, Christina,Rothfelder, Robin,Scott, Daniel J.,Fischer, Tillmann G.,Zeitler, Kirsten,Wolf, Robert
supporting information, p. 16374 - 16382 (2020/11/03)
Asymmetrically substituted tertiary phos...
6372-42-5 Process route
-
-
13689-20-8
(cyclohexyl)diphenylphosphane oxide
-
-
6372-42-5
cyclohexyldiphenylphosphine
| Conditions | Yield |
|---|---|
|
With
copper(II) trifluoromethanesulfonate; 1,1,3,3-Tetramethyldisiloxane;
In
toluene;
at 100 ℃;
Inert atmosphere;
|
86% |
|
With
oxalyl dichloride; hydrogen;
In
chloroform-d1;
at 130 ℃;
for 18h;
under 60006 Torr;
Reagent/catalyst;
|
85% |
|
(cyclohexyl)diphenylphosphane oxide;
With
trifluoroacetic anhydride;
In
1,4-dioxane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
15-crown-5; sodium hydride; sodium hydrogencarbonate;
In
1,4-dioxane;
at 150 ℃;
for 24h;
Inert atmosphere;
|
85% |
|
With
copper(II) bis(trifluoromethanesulfonate); 1,1,3,3-tetramethyldisilazane;
In
toluene;
at 80 ℃;
|
82% |
|
With
copper(II) bis(trifluoromethanesulfonate); 1,1,3,3-tetramethyldisilazane;
In
toluene;
at 80 ℃;
|
82% |
|
With
triphenyl phosphite; diphenyl hydrogen phosphite; iodine;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
|
75% |
|
With
oxalyl dichloride; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; triethylamine;
In
dichloromethane;
at 40 ℃;
for 2h;
Inert atmosphere;
|
73% |
|
With
diethoxymethylane; Bis(p-nitrophenyl) phosphate;
In
toluene;
at 110 ℃;
chemoselective reaction;
Inert atmosphere;
|
70% |
|
With
aluminum (III) chloride; N,N,N,N,-tetramethylethylenediamine; tetrabutyl-ammonium chloride; tert-butylammonium hexafluorophosphate(V);
In
acetonitrile;
at -20 ℃;
Inert atmosphere;
Glovebox;
Electrolysis;
|
45% |
|
(cyclohexyl)diphenylphosphane oxide;
With
[Fe(CO)(1,3-bis(diphenylphosphino)propane)H(NO)]; phenylsilane; N-ethyl-N,N-diisopropylamine;
In
toluene;
at 100 ℃;
for 18h;
Schlenk technique;
With
sodium hydroxide;
In
methanol; water; toluene;
at 20 ℃;
for 1h;
chemoselective reaction;
Schlenk technique;
|
44% |
|
With
indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane;
In
toluene;
at 100 ℃;
for 22h;
Inert atmosphere;
Sealed tube;
|
-
-
1079-66-9,74391-44-9
chloro-diphenylphosphine
-
-
126812-30-4
1,3-dioxoisoindolin-2-yl cyclohexanecarboxylate
-
-
6372-42-5
cyclohexyldiphenylphosphine
| Conditions | Yield |
|---|---|
|
With
N,N,N',N'',N'''-pentamethyldiethylenetriamine; zinc;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
Reagent/catalyst;
Time;
|
95% |
6372-42-5 Upstream products
-
108-85-0
1-bromocyclohexane
-
603-35-0
triphenylphosphine
-
542-18-7
cyclohexyl chloride
-
15658-08-9
dicyclohexylzinc(II)
6372-42-5 Downstream products
-
63699-00-3
Dichlor(cyclohexyl)diphenylphosphoran
-
72144-83-3
1,4-di(cyclohexylphenylphosphino)butane
-
13689-20-8
(cyclohexyl)diphenylphosphane oxide
-
36293-82-0
cyclohexyl(methyl)phenylphosphine
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