668983-97-9

  • Product Name:Dibenzothiophene-2-boronic Acid
  • Molecular Formula:C12H9BO2S
  • Purity:99%
  • Molecular Weight:228.079
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Product Details;

CasNo: 668983-97-9

Molecular Formula: C12H9BO2S

factory and supplier 668983-97-9 Dibenzothiophene-2-boronic Acid in stock

  • Molecular Formula:C12H9BO2S
  • Molecular Weight:228.079
  • Vapor Pressure:4.97E-10mmHg at 25°C 
  • Refractive Index:1.738 
  • Boiling Point:480.2 °C at 760 mmHg 
  • PKA:8.39±0.30(Predicted) 
  • Flash Point:244.2 °C 
  • PSA:68.70000 
  • Density:1.38 g/cm3 
  • LogP:1.73430 

DIBENZOTHIOPHENE-2-BORONIC ACID(Cas 668983-97-9) Usage

InChI:InChI=1/C12H9BO2S/c14-13(15)8-5-6-12-10(7-8)9-3-1-2-4-11(9)16-12/h1-7,14-15H

668983-97-9 Relevant articles

Electrochemical Synthesis of Biaryls via Oxidative Intramolecular Coupling of Tetra(hetero)arylborates

Music, Arif,Baumann, Andreas N.,Spie?, Philipp,Plantefol, Allan,Jagau, Thomas C.,Didier, Dorian

supporting information, p. 4341 - 4348 (2020/03/04)

We report herein versatile, transition m...

Bending-Type Electron Donor-Donor-Acceptor Triad: Dual Excited-State Charge-Transfer Coupled Structural Relaxation

Lin, Jia-An,Li, Shu-Wei,Liu, Zong-Ying,Chen, Deng-Gao,Huang, Chun-Ying,Wei, Yu-Chen,Chen, Yi-Yun,Tsai, Zheng-Hua,Lo, Chun-Yuan,Hung, Wen-Yi,Wong, Ken-Tsung,Chou, Pi-Tai

, p. 5981 - 5992 (2019/08/27)

The triad types of molecules with variou...

COMPOUND FOR ORGANIC ELECTRONIC ELEMENT, ORGANIC ELECTRONIC ELEMENT USING THE SAME, AND A ELECTRONIC DEVICE THEREOF

-

Paragraph 0142-0145, (2019/01/30)

The present invention provides a novel c...

NOVEL TRIAZINE COMPOUND, AND ORGANIC ELECTRONIC ELEMENT AND PLANT-GROWING LIGHTING THAT USE THE SAME

-

Paragraph 0076, (2018/07/28)

PROBLEM TO BE SOLVED: To provide a triaz...

668983-97-9 Process route

2-bromodibenzothiophene
22439-61-8

2-bromodibenzothiophene

dibenzo[b,d]thien-2-ylboronic acid
668983-97-9

dibenzo[b,d]thien-2-ylboronic acid

Conditions
Conditions Yield
2-bromodibenzothiophene; With n-butyllithium; In tetrahydrofuran; hexane; toluene; at -70 ℃; for 1h; Inert atmosphere;
With Triisopropyl borate; In tetrahydrofuran; hexane; toluene; at 20 ℃; for 6h;
With hydrogenchloride; In tetrahydrofuran; hexane; water; toluene; for 0.5h;
95%
2-bromodibenzothiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;
With Triisopropyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h;
92%
With n-butyllithium; Trimethyl borate; sulfuric acid; water; In hexane; at -78 - 20 ℃;
88%
With n-butyllithium; diethyl ether; Behandeln des Reaktionsprodukts mit Triisopropylborat in Aether bei -60grad und Behandeln des Reaktionsgemisches mit Wasser;
2-bromodibenzothiophene
22439-61-8

2-bromodibenzothiophene

Trimethyl borate
121-43-7,63156-11-6

Trimethyl borate

dibenzo[b,d]thien-2-ylboronic acid
668983-97-9

dibenzo[b,d]thien-2-ylboronic acid

Conditions
Conditions Yield
2-bromodibenzothiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;
Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h;
82%
2-bromodibenzothiophene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
Trimethyl borate; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
With hydrogenchloride; In tetrahydrofuran; water; for 0.5h; Inert atmosphere;
80%
2-bromodibenzothiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;
Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h;
2-bromodibenzothiophene; With n-butyllithium;
Trimethyl borate;
With hydrogenchloride;

668983-97-9 Upstream products

  • 22439-61-8
    22439-61-8

    2-bromodibenzothiophene

  • 132-65-0
    132-65-0

    dibenzothiophene

  • 5419-55-6
    5419-55-6

    Triisopropyl borate

  • 1776-66-5
    1776-66-5

    triisopropylborane

668983-97-9 Downstream products

  • 1398393-70-8
    1398393-70-8

    C44H27N3S

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