1153-85-1
- Product Name：3-bromo-9-phenyl-9H-carbazole
- Molecular Formula：C18H12BrN
- Purity：99%
- Molecular Weight：322.204
Product Details;
CasNo： 1153-85-1
Molecular Formula： C18H12BrN
factory and supplier 1153-85-1 3-bromo-9-phenyl-9H-carbazole in stock
- Molecular Formula:C18H12BrN
- Molecular Weight:322.204
- Vapor Pressure:1.05E-08mmHg at 25°C
- Melting Point:98 °C
- Refractive Index:1.672
- Boiling Point:461.7 °C at 760 mmHg
- Flash Point:233 °C
- PSA：4.93000
- Density:1.39 g/cm3
- LogP:5.54620
3-Bromo-9-phenylcarbazole(Cas 1153-85-1) Usage
InChI:InChI=1/C18H12BrN/c19-13-10-11-18-16(12-13)15-8-4-5-9-17(15)20(18)14-6-2-1-3-7-14/h1-12H
1153-85-1 Relevant articles
Pyridyl Pyrrolide Boron Complexes: The Facile Generation of Thermally Activated Delayed Fluorescence and Preparation of Organic Light-Emitting Diodes
Shiu, Yi-Jiun,Cheng, Yung-Chen,Tsai, Wei-Lung,Wu, Chung-Chih,Chao, Chun-Tien,Lu, Chin-Wei,Chi, Yun,Chen, Yi-Ting,Liu, Shih-Hung,Chou, Pi-Tai
, p. 3017 - 3021 (2016)
The electron positive boron atom usually...
Novel bifluorene based conjugated systems: Synthesis and properties
Grisorio, Roberto,Dell'Aquila, Antonio,Romanazzi, Giuseppe,Suranna, Gian Paolo,Mastrorilli, Piero,Cosma, Pynalisa,Acierno, Domenico,Amendola, Eugenio,Ciccarella, Giuseppe,Nobile, Cosimo Francesco
, p. 627 - 634 (2006)
A series of novel bifluorene based syste...
Efficient thermally activated delayed fluorescence of functional phenylpyridinato boron complexes and high performance organic light-emitting diodes
Shiu, Yi-Jiun,Chen, Yi-Ting,Lee, Wei-Kai,Wu, Chung-Chih,Lin, Tzu-Chieh,Liu, Shih-Hung,Chou, Pi-Tai,Lu, Chin-Wei,Cheng, I-Chen,Lien, Yi-Jyun,Chi, Yun
, p. 1452 - 1462 (2017)
A new series of functional phenylpyridin...
Imidazolyl-Phenylcarbazole-Based Host Materials and Their Use for Co-host Designs in Phosphorescent OLEDs
Yi, Rong-Huei,Lei, Ya-Chun,Tseng, Yeh-Hsiang,Lin, Yi-Fan,Cheng, Yen-Chia,Fang, Yu-Chuan,Ho, Cheng-Yung,Tsai, Wei-Wen,Chang, Chih-Hao,Lu, Chin-Wei
, (2021/12/06)
In recent years, owing to the demand for...
Thiophene ethylene malononitrile structural compound and preparation method thereof
-
Paragraph 0069-0071, (2021/04/28)
The invention discloses a thiophene ethy...
Preparation method of 3 - bromo - N - phenyl carbazole
-
Paragraph 0024; 0032-0038; 0039; 0047-0053, (2021/10/11)
The invention relates to a preparation m...
Nitrogen-containing compound, electronic element and electronic device
-
Paragraph 0176-0180, (2021/01/29)
The invention belongs to the technical f...
1153-85-1 Process route
-
-
1592-95-6
3-bromo-9H-carbazole
-
-
591-50-4
iodobenzene
-
-
1153-85-1
3-bromo-9-phenyl-9H-carbazole
| Conditions | Yield |
|---|---|
|
3-bromo-9H-carbazole; iodobenzene;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
With
copper(l) iodide;
In
N,N-dimethyl-formamide;
at 100 ℃;
|
93% |
|
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 10h;
Inert atmosphere;
|
89.7% |
|
With
18-crown-6 ether; copper; potassium carbonate;
In
1,2-dichloro-benzene;
at 180 ℃;
for 24h;
|
88% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tributylphosphine;
In
toluene;
for 12h;
Heating;
|
87.22% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
|
86% |
|
With
copper(l) iodide; 1,10-Phenanthroline; potassium carbonate;
In
5,5-dimethyl-1,3-cyclohexadiene;
for 6h;
Reflux;
|
86% |
|
3-bromo-9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide;
for 1h;
iodobenzene;
In
N,N-dimethyl-formamide;
|
86% |
|
With
copper(l) iodide; 1,10-Phenanthroline; 18-crown-6 ether; potassium carbonate;
In
N,N-dimethyl-formamide;
at 150 ℃;
for 8h;
Inert atmosphere;
|
85.5% |
|
With
copper; potassium carbonate; sodium sulfate;
In
nitrobenzene;
at 195 ℃;
|
82% |
|
With
copper; potassium carbonate;
In
nitrobenzene;
for 16h;
Inert atmosphere;
Reflux;
|
81% |
|
With
copper; potassium carbonate;
In
nitrobenzene;
for 16h;
Inert atmosphere;
Reflux;
|
81% |
|
With
copper; potassium carbonate; sodium sulfate;
In
nitrobenzene;
at 200 ℃;
|
79% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
for 24h;
|
78% |
|
With
potassium carbonate; copper dichloride;
In
dimethyl sulfoxide;
for 12h;
Reflux;
|
76% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
|
75% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
|
75% |
|
With
copper; potassium carbonate; sodium sulfate;
In
nitrobenzene;
at 200 ℃;
|
73% |
|
With
copper; potassium carbonate; sodium sulfate;
In
nitrobenzene;
at 200 ℃;
|
72% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
for 6h;
Inert atmosphere;
Reflux;
|
65% |
|
With
18-crown-6 ether; copper; sodium t-butanolate;
In
toluene;
at 100 ℃;
for 24h;
|
57% |
|
With
18-crown-6 ether; copper; sodium t-butanolate;
In
toluene;
at 100 ℃;
for 24h;
|
57% |
|
With
copper(I) oxide; 2,2,6,6-tetramethylheptane-3,5-dione; potassium hydroxide;
In
N,N-dimethyl-formamide;
at 130 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
|
54% |
|
With
copper(l) iodide;
Inert atmosphere;
|
|
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
for 8h;
|
|
|
iodobenzene;
With
tri-tert-butyl phosphine; palladium diacetate;
In
toluene;
at 20 ℃;
for 1h;
Inert atmosphere;
3-bromo-9H-carbazole;
With
potassium carbonate;
In
toluene;
at 80 ℃;
for 6h;
Inert atmosphere;
|
1.9 g |
|
With
copper(l) iodide;
Inert atmosphere;
|
|
|
With
copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide;
In
5,5-dimethyl-1,3-cyclohexadiene;
|
-
-
108-86-1,52753-63-6
bromobenzene
-
-
1592-95-6
3-bromo-9H-carbazole
-
-
1153-85-1
3-bromo-9-phenyl-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
dibenzo-18-crown-6; potassium acetate; copper;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 4h;
|
71% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
at 100 ℃;
for 24h;
|
1153-85-1 Upstream products
-
1150-62-5
N-phenylcarbazole
-
591-50-4
iodobenzene
-
86-74-8
9H-carbazole
-
13716-12-6
tri-tert-butyl phosphine
1153-85-1 Downstream products
-
854952-58-2
N-phenyl-9H-carbazol-3-boronic acid
-
922721-28-6
9-phenyl-3-(pyridin-2-yl)-9H-carbazole
-
918137-84-5
6-bromo-9,9'-diphenyl-9H,9'H-3,3'-bicarbazole
-
918137-86-7
(9,9'-diphenyl-9H,9'H-[3,3'-biscarbazol]-6-yl)boronic acid
Relevant Products
-
5-Bromoindole-2-carboxylic acidCAS：7254-19-5
-
9-phenylcarbazoleCAS：1150-62-5
-
Methyl 3-hydroxy-4-nitrobenzoateCAS：713-52-0
