62932-94-9

  • Product Name:2-Bromo-4-hydroxy-3-(hydroxymethyl)acetophenone
  • Molecular Formula:C9H9BrO3
  • Purity:99%
  • Molecular Weight:245.073
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Product Details;

CasNo: 62932-94-9

Molecular Formula: C9H9BrO3

factory and supplier 62932-94-9 2-Bromo-4-hydroxy-3-(hydroxymethyl)acetophenone in stock

  • Molecular Formula:C9H9BrO3
  • Molecular Weight:245.073
  • Melting Point:128-131°C 
  • Boiling Point:349.4±11.0 °C(Predicted) 
  • PKA:7.69±0.20(Predicted) 
  • PSA:57.53000 
  • Density:1.674±0.06 g/cm3(Predicted) 
  • LogP:1.46210 

2-BROMO-1-[4-HYDROXY-3-(HYDROXYMETHYL)PHENYL]ETHAN-1-ONE(Cas 62932-94-9) Usage

Preparation

Obtained by treatment of its diacetate with 1 N hydrogen bromide in tetrahydrofuran at 75°.

InChI:InChI=1S/C9H9BrO3/c10-4-9(13)6-1-2-8(12)7(3-6)5-11/h1-3,11-12H,4-5H2

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62932-94-9 Process route

3'-acetoxymethyl-4'-acetoxy-2-bromoacetophenone
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2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
62932-94-9

2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone

Conditions
Conditions Yield
With hydrogen bromide; In tetrahydrofuran; at 75 ℃;
With hydrogen bromide; In methanol; water;
With hydrogen bromide; In methanol; water;
4'-acetoxy-3'-(acetoxymethyl)acetophenone
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2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone
62932-94-9

2-bromo-1-[4-hydroxy-3-(hydroxymethyl)-phenyl]ethanone

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: polyvinylpyridinium bromide perbromide resin / CH2Cl2
2: 1N HBr / tetrahydrofuran / 75 °C
With polyvinylpyridinium bromide perbromide resin; hydrogen bromide; In tetrahydrofuran; dichloromethane;

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