2632-99-7
- Product Name：4,4'-Azobispyridine
- Molecular Formula：C10H8N4
- Purity：99%
- Molecular Weight：184.2
Product Details;
CasNo： 2632-99-7
Molecular Formula： C10H8N4
factory and supplier 2632-99-7 4,4'-Azobispyridine in stock
- Molecular Formula:C10H8N4
- Molecular Weight:184.2
- Melting Point:96-101°C
- Boiling Point:344.9 °C at 760 mmHg
- PKA:1.93±0.10(Predicted)
- Flash Point:162.4 °C
- PSA：50.50000
- Density:1.18 g/cm3
- LogP:2.89200
2632-99-7 Relevant articles
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Sahoo, Rupam,Chand, Santanu,Mondal, Manas,Pal, Arun,Pal, Shyam Chand,Rana, Malay Kumar,Das, Madhab C.
, p. 12624 - 12631 (2020)
The design and construction of “thermody...
Control over catenation in metal-organic frameworks via rational design of the organic building block
Farha, Omar K.,Malliakas, Christos D.,Kanatzidis, Mercouri G.,Hupp, Joseph T.
, p. 950 - 952 (2010)
(Chemical Equation Presented) Metal-orga...
Synthesis and characterization of four novel manganese(II) chains formed by 4,4′-azobis(pyridine) and benzoate or nitrobenzoates: Stabilization of unusual ladder structures
Kar, Paramita,Drew, Michael G.B.,Gómez-García, Carlos J.,Ghosh, Ashutosh
, p. 229 - 239 (2013)
Four new manganese(II) coordination poly...
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, (2020)
Two azo functionalized Zn(II)-based MOFs...
4-Pyridylnitrene and 2-pyrazinylcarbene
Wentrup, Curt,Reisinger, Ales,Kvaskoff, David
, p. 754 - 760 (2013)
Both flash vacuum thermolysis (FVT) and ...
Bifunctional Cs?Au/Co3O4 (Basic and Redox)-Catalyzed Oxidative Synthesis of Aromatic Azo Compounds from Anilines
Oseghale, Charles O.,Fapojuwo, Dele Peter,Alimi, Oyekunle Azeez,Akinnawo, Christianah Aarinola,Mogudi, Batsile M.,Onisuru, Oluwatayo Racheal,Meijboom, Reinout
supporting information, p. 5063 - 5073 (2021/09/30)
An eco-friendly alkali-promoted (Cs?Au/C...
Electrochemical dehydrogenation of hydrazines to azo compounds
Du, Ke-Si,Huang, Jing-Mei
, p. 1680 - 1685 (2019/04/08)
A strategy for the electrochemical dehyd...
2632-99-7 Process route
-
-
504-24-5
4-aminopyridine
-
-
2632-99-7
1,2-bis(5-methylisoxazol-3-yl)hydrazine
| Conditions | Yield |
|---|---|
|
With
sodium hypochlorite;
In
water;
at 0 ℃;
for 0.5h;
|
64% |
|
With
sodium hypochlorite;
In
water;
at 0 - 5 ℃;
for 1.5h;
|
64% |
|
With
pyridine; sodium hypochlorite;
In
water;
at 0 - 5 ℃;
|
51% |
|
With
sodium hypochlorite solution;
In
water;
at 0 - 5 ℃;
for 0.5h;
Cooling with ice;
|
51% |
|
With
Cs+promoted 1% Au on Co3O4; air;
In
toluene;
at 100 ℃;
for 18h;
under 760.051 Torr;
Green chemistry;
|
35% |
|
With
sodium hypochlorite;
In
water;
at 0 ℃;
for 0.5h;
|
|
|
With
sodium perchlorate;
In
water;
at 0 ℃;
|
|
|
With
sodium hypochlorite;
|
|
|
With
sodium hypochlorite;
In
water;
at 0 ℃;
for 1h;
|
|
|
Multi-step reaction with 2 steps
1.1: sodium hypochlorite / water / 1 h / 0 °C
1.2: 4 h / 60 °C
2.1: sodium acetate / ethanol / 20 °C / Electrolysis; Green chemistry
With
sodium hypochlorite; sodium acetate;
In
ethanol; water;
|
|
|
With
sodium hypochlorite;
|
-
-
19808-51-6
1,2-di(pyridin-4-yl)hydrazine
-
-
2632-99-7
1,2-bis(5-methylisoxazol-3-yl)hydrazine
| Conditions | Yield |
|---|---|
|
With
sodium acetate;
In
ethanol;
at 20 ℃;
Electrolysis;
Green chemistry;
|
83% |
|
With
[bis(acetoxy)iodo]benzene;
In
dimethyl sulfoxide;
at 20 ℃;
for 6h;
|
73% |
|
With
[bis(acetoxy)iodo]benzene;
In
dimethyl sulfoxide;
at 20 ℃;
for 6h;
|
69% |
|
With
[bis(acetoxy)iodo]benzene;
In
dimethyl sulfoxide;
at 20 ℃;
for 7h;
|
2632-99-7 Upstream products
-
119416-31-8
[4,4']azoxypyridine
-
504-24-5
4-aminopyridine
-
1122-61-8
4-nitropyridine
-
1124-33-0
4-nitraminopyridine N-oxide
2632-99-7 Downstream products
-
19808-51-6
1,2-di(pyridin-4-yl)hydrazine
-
1282616-25-4
trans-[(4,4'-azobispyridine)(Au(C6F4OCH2C6H4O(CH2)11CH3-p))2]
-
1282616-23-2
trans-[(4,4'-azobispyridine)(Au(C6F4O(CH2)11CH3-p))2]
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