16807-13-9

  • Product Name:3-Iodo-9H-carbazole
  • Molecular Formula:C12H8IN
  • Purity:99%
  • Molecular Weight:293.107
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Product Details;

CasNo: 16807-13-9

Molecular Formula: C12H8IN

factory and supplier 16807-13-9 3-Iodo-9H-carbazole in stock

  • Molecular Formula:C12H8IN
  • Molecular Weight:293.107
  • Melting Point:195-197℃ 
  • Boiling Point:430.6±18.0 °C(Predicted) 
  • PKA:16.54±0.30(Predicted) 
  • Density:1.854 

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16807-13-9 Process route

9H-carbazole
86-74-8,105184-46-1,97960-57-1

9H-carbazole

3-iodocarbazole
16807-13-9

3-iodocarbazole

Conditions
Conditions Yield
With N-iodo-succinimide; In acetic acid; at 20 ℃;
97%
9H-carbazole; With N-iodo-succinimide; acetic acid; at 20 ℃; for 12h;
With sodium hydrogencarbonate; In water; ethyl acetate;
97%
With iodine; In dimethyl sulfoxide; at 110 ℃; for 6h; Temperature; Concentration; regioselective reaction;
95%
With N-iodo-succinimide; In acetic acid; at 20 ℃; for 1h;
86%
With diphenyliodonium tetrafluoroborate; copper(II) sulfate; In acetonitrile; at 65 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;
79%
With [bis(pyridine)iodine]+ tetrafluoroborate; copper(II) sulfate; In acetonitrile; at 65 ℃; for 0.166667h; Inert atmosphere;
79%
With potassium iodate; potassium carbonate; acetic acid; potassium iodide; at 80 ℃; for 5h;
72%
9H-carbazole; With acetic acid; potassium iodide; at 110 ℃;
With potassium iodate; at 100 ℃; for 0.166667h;
72.7%
With iodine; silver nitrate; acetic acid; at 20 ℃;
70%
9H-carbazole; With potassium iodide; In acetic acid; at 100 ℃; for 1h;
With potassium iodate; In acetic acid; at 100 ℃; for 2h;
70%
With iron(III) chloride; sodium iodide; In acetonitrile; for 8h;
68%
9H-carbazole; With acetic acid; potassium iodide; at 85 ℃; Reflux;
With potassium iodate; at 85 ℃; for 0.166667h;
62%
With sodium periodate; sulfuric acid; iodine; In ethanol; at 60 ℃; for 2h;
49%
With sodium periodate; sulfuric acid; iodine; In isopropyl alcohol; at 65 ℃; for 6h;
48%
With potassium iodate; potassium iodide; In acetic acid; at 45 ℃;
47%
9H-carbazole; With ammonium iodide; In methanol; for 0.0333333h;
In methanol; at 75 ℃;
47%
With potassium iodate; potassium iodide; In acetic acid; for 0.166667h; Reflux;
45%
With potassium iodate; acetic acid; potassium iodide; for 0.166667h; Reflux;
45%
With potassium iodate; acetic acid; potassium iodide; Heating;
44.3%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With N-iodo-succinimide; acetic acid; at 20 ℃; for 5h; Inert atmosphere;
44%
With potassium iodate; acetic acid; potassium iodide; at 100 ℃; for 2h;
40%
With potassium iodate; acetic acid; potassium iodide; at 85 ℃; for 0.166667h;
39%
With periodic acid dihydrate; sulfuric acid; iodine; In ethanol; at 20 ℃; for 4h;
18.8%
With potassium iodate; acetic acid; potassium iodide; at 80 ℃; for 1h;
15%
With potassium iodate; potassium iodide;
With sulfuric acid; iodine; periodic acid; acetic acid; In water; at 70 ℃; for 1h;
With potassium iodate; potassium iodide;
With potassium iodate; potassium iodide; In acetic acid;
With sulfuric acid; iodine; periodic acid; In water; acetic acid; at 70 ℃; for 1h;
With potassium iodate; potassium iodide; In acetic acid; at 50 ℃; for 2h;
With potassium iodate; acetic acid; potassium iodide;
With Iodine monochloride; In acetonitrile; at 0 - 20 ℃; for 4h; Inert atmosphere;
With potassium iodate; acetic acid; potassium iodide;
With potassium iodate; potassium iodide;
With Iodine monochloride; at 0 - 20 ℃; for 4h;
With potassium iodate; potassium iodide;
With Iodine monochloride; In acetonitrile; at 0 - 20 ℃; for 4h; Inert atmosphere;
With potassium iodate; acetic acid; potassium iodide; Reflux;
With periodic acid dihydrate; sulfuric acid; iodine; In ethanol; water; for 4h;
5.1 g
With potassium iodate; potassium iodide; In acetic acid; for 0.333333h; Reflux;
With potassium iodate; potassium iodide;
With potassium iodate; acetic acid; potassium iodide; at 120 ℃; for 0.166667h;
With potassium iodate; potassium iodide; at 130 ℃;
With sodium periodate; sulfuric acid; iodine; In ethanol;
With sodium periodate; sulfuric acid; iodine; In ethanol;
With potassium iodate; acetic acid; potassium iodide; Reflux;
With potassium iodate; acetic acid; potassium iodide; at 110 ℃; for 2h;
3-iodo-9-(p-tolylsulfonyl)carbazole
861312-65-4

3-iodo-9-(p-tolylsulfonyl)carbazole

3-iodocarbazole
16807-13-9

3-iodocarbazole

Conditions
Conditions Yield
With sodium hydride; In N,N-dimethyl acetamide; at 60 ℃; for 3.5h; Inert atmosphere;
85%

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