57103-02-3
- Product Name：3,6-Diiodo-9H-carbazole
- Molecular Formula：C12H7I2N
- Purity：99%
- Molecular Weight：419.003
Product Details;
CasNo： 57103-02-3
Molecular Formula： C12H7I2N
factory and supplier 57103-02-3 3,6-Diiodo-9H-carbazole in stock
- Molecular Formula:C12H7I2N
- Molecular Weight:419.003
- Melting Point:205.0 to 209.0 °C
- Boiling Point:498.3±25.0 °C(Predicted)
- PKA:15.68±0.30(Predicted)
- PSA：15.79000
- Density:2.326±0.06 g/cm3(Predicted)
- LogP:4.53030
57103-02-3 Relevant articles
(Bi)phenyl substituted 9-(2,2-diphenylvinyl)carbazoles as low cost hole transporting materials for efficient red PhOLEDs
Grigalevicius, Saulius,Tavgeniene, Daiva,Krucaite, Gintare,Griniene, Raimonda,Wang, Yen-Po,Tsai, Shang-Ru,Chang, Chih-Hao
, p. 173 - 178 (2018/06/26)
Two low-cost 9-(2,2-diphenylvinyl)carbaz...
Easy accessible blue luminescent carbazole-based materials for organic light-emitting diodes
Reig, Marta,Gozálvez, Cristian,Bujaldón, Roger,Bagdziunas, Gintautas,Ivaniuk, Khrystyna,Kostiv, Nataliya,Volyniuk, Dmytro,Grazulevicius, Juozas V.,Velasco, Dolores
, p. 24 - 35 (2016/10/11)
The thermal, optical, electrochemical an...
Solution-processable naphthalene and phenyl substituted carbazole core based hole transporting materials for efficient organic light-emitting diodes
Kumar, Sudhir,An, Chih-Chia,Sahoo, Snehasis,Griniene, Raimonda,Volyniuk, Dmytro,Grazulevicius, Juozas V.,Grigalevicius, Saulius,Jou, Jwo-Huei
, p. 9854 - 9864 (2017/10/13)
Solution-processable molecular hole tran...
A one-pot direct iodination of the Fischer-Borsche ring using molecular iodine and its utility in the synthesis of 6-oxygenated carbazole alkaloids
Naykode, Mahavir S.,Humne, Vivek T.,Lokhande, Pradeep D.
, p. 2392 - 2396 (2015/05/04)
An efficient regioselective iodination o...
57103-02-3 Process route
-
-
86-74-8,105184-46-1,97960-57-1
9H-carbazole
-
-
16807-13-9
3-iodocarbazole
-
-
57103-02-3
3,6-diiodocarbazole
| Conditions | Yield |
|---|---|
|
9H-carbazole;
With
sodium periodate; sulfuric acid; iodine;
In
ethanol;
at 65 ℃;
for 1h;
With
sodium hydroxide;
In
ethanol;
|
70% 7.5% |
|
9H-carbazole;
With
sodium periodate; sulfuric acid; iodine;
In
ethanol;
at 65 ℃;
for 1h;
With
sodium hydroxide;
In
ethanol;
|
70% 7.5% |
|
With
iodine;
In
dimethyl sulfoxide;
at 110 ℃;
for 10h;
regioselective reaction;
|
60% 30% |
|
With
potassium iodate; acetic acid; potassium iodide;
for 0.166667h;
Reflux;
|
42.1% 40% |
|
With
potassium iodate; acetic acid; potassium iodide;
|
|
|
With
trifluorormethanesulfonic acid; [bis(pyridine)iodine]+ tetrafluoroborate;
In
dichloromethane;
at 25 ℃;
for 20h;
Product distribution;
|
|
|
With
potassium iodate; acetic acid; potassium iodide;
Reflux;
|
|
|
With
potassium iodate; acetic acid; potassium iodide;
|
|
|
With
potassium iodate; acetic acid; potassium iodide;
|
-
-
86-74-8,105184-46-1,97960-57-1
9H-carbazole
-
-
16807-13-9
3-iodocarbazole
-
-
57103-02-3
3,6-diiodocarbazole
-
-
1,6-diiodocarbazole
| Conditions | Yield |
|---|---|
|
With
sodium periodate; sulfuric acid; potassium iodide;
In
ethanol;
at 65 ℃;
for 1.21667h;
|
72 % Chromat. 14 % Chromat. 15 % Chromat. |
57103-02-3 Upstream products
-
86-74-8
9H-carbazole
-
64-19-7
acetic acid
-
1592-95-6
3-bromo-9H-carbazole
-
100-44-7
benzyl chloride
57103-02-3 Downstream products
-
606129-89-9
9-acetyl-3,6-diiodo carbazole
-
78932-83-9
3,6-di((E)-styryl)-9H-carbazole
-
62913-24-0
3,6-bis(2-phenylethynyl)-9H-carbazole
-
56525-79-2
3,6-diphenylcarbazole
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