66197-72-6
- Product Name：BroMoMethyl -phosphonic acid diethyl ester
- Molecular Formula：C5H12BrO3P
- Purity：99%
- Molecular Weight：231.026
Product Details;
CasNo： 66197-72-6
Molecular Formula： C5H12BrO3P
factory and supplier 66197-72-6 BroMoMethyl -phosphonic acid diethyl ester in stock
- Molecular Formula:C5H12BrO3P
- Molecular Weight:231.026
- Boiling Point:99 °C(Press: 1 Torr)
- PSA：45.34000
- Density:1.4474 g/cm3
- LogP:2.60490
66197-72-6 Relevant articles
Enantioselective organocatalytic conjugate addition of aldehydes to vinyl sulfones and vinyl phosphonates as challenging michael acceptors
Sulzer-Mosse, Sarah,Alexakis, Alexandre,Mareda, Jiri,Bollot, Guillaume,Bernardinelli, Gerald,Filinchuk, Yaroslav
supporting information; experimental part, p. 3204 - 3220 (2009/12/03)
Chiral amines with a pyrrolidine framewo...
Free radical reaction of α-haloalkylphosphonates with alkenes and alkynes: A new approach to modified phosphonates
Balczewski,Mikolajczyk
, p. 392 - 396 (2007/10/02)
A new approach to the synthesis of phosp...
Improved preparation of diethyl bromomethylphosphonate and diiodomethane-catalyzed triethylphosphite Michaelis-Arbuzov isomerization
Ezquerra,Yruretagoyena,Moreno-Manas,Roglans
, p. 191 - 194 (2007/10/02)
An improved method to prepare diethyl br...
α-Substituted Phosphonates. 39. Methane-diphosphonic Esters by U.V.-Induced Michaelis-Becker-Reaction
Czekanski, T.,Gross, H.,Costisella, B.
, p. 537 - 544 (2007/10/02)
Dibromomethane resp. chlorbromomethane r...
66197-72-6 Process route
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-
762-04-9
phosphonic acid diethyl ester
-
-
74-95-3
1,1-dibromomethane
-
-
78-38-6
ethylphosphonic acid diethyl ester
-
-
66197-72-6
diethyl (bromomethyl)phosphonate
-
-
1660-94-2
Tetraethyl methylenediphosphonate
| Conditions | Yield |
|---|---|
|
at 140 - 150 ℃;
for 4h;
Yield given. Yields of byproduct given;
glass ampoule;
|
-
-
122-52-1
triethyl phosphite
-
-
74-95-3
1,1-dibromomethane
-
-
78-38-6
ethylphosphonic acid diethyl ester
-
-
66197-72-6
diethyl (bromomethyl)phosphonate
-
-
1660-94-2
Tetraethyl methylenediphosphonate
| Conditions | Yield |
|---|---|
|
for 48h;
Reflux;
|
56% |
66197-72-6 Upstream products
-
122-52-1
triethyl phosphite
-
74-95-3
1,1-dibromomethane
-
762-04-9
phosphonic acid diethyl ester
66197-72-6 Downstream products
-
1660-94-2
Tetraethyl methylenediphosphonate
-
58263-57-3
O,O-diethyl, diphenylmethylenephosphonophosphinate
-
33512-26-4
diethyl (phthalimidomethyl)phosphonate
-
683-08-9
Diethyl methylphosphonate
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-
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