1484-13-5
- Product Name：N-ethylenecarbazole
- Molecular Formula：C14H11N
- Purity：99%
- Molecular Weight：193.248
Product Details;
CasNo： 1484-13-5
Molecular Formula： C14H11N
Appearance： slightly brown crystalline solid
factory and supplier 1484-13-5 N-ethylenecarbazole in stock
- Molecular Formula:C14H11N
- Molecular Weight:193.248
- Appearance/Colour:slightly brown crystalline solid
- Vapor Pressure:0mmHg at 25°C
- Melting Point:60-65 °C
- Refractive Index:1.77
- Boiling Point:328.5 °C at 760 mmHg
- Flash Point:152.5 °C
- PSA：4.93000
- Density:1.05 g/cm3
- LogP:3.89500
9-Vinylcarbazole(Cas 1484-13-5) Usage
|
Purification Methods |
Crystallise N-vinylcarbazole repeatedly from MeOH in amber glassware. It sublimes in a vacuum. [Beilstein 20 II 282, 20 III/IV 3830, 20/8 V 19.] |
InChI:InChI=1/C14H11N/c1-2-10-6-5-8-12-11-7-3-4-9-13(11)15-14(10)12/h2-9,15H,1H2
1484-13-5 Relevant articles
Substrate-Controlled Regio- and Stereoselective Synthesis of (Z)- and (E)- N-Styrylated Carbazoles, Aza-carbazoles, and γ-Carbolines via Hydroamination of Alkynes
Garg, Vineeta,Kumar, Pradeep,Verma, Akhilesh K.
, p. 11686 - 11702 (2018)
We report herein the substrate-controlle...
Vinylation of a secondary amine core with calcium carbide for efficient post-modification and access to polymeric materials
Rodygin, Konstantin S.,Bogachenkov, Alexander S.,Ananikov, Valentine P.
, (2018)
We developed a simple and efficient stra...
Reactions of carbazole with dimethyl alkanedisulfonates
Sokolov,Aksinenko, A. Yu.,Epishina,Goreva
, (2017)
Reaction of carbazole with dimethyl alka...
Phosphine-Catalyzed Vinylation at Low Acetylene Pressure
Bienewald, Frank,Comba, Peter,Hashmi, A. Stephen K.,Menche, Maximilian,Rominger, Frank,Schafer, Ansgar,Schaub, Thomas,Sitte, Nikolai A.,Tuzina, Pavel
, p. 13041 - 13055 (2021/09/18)
The vinylation of various nucleophiles w...
Base-Mediated Site-Selective Hydroamination of Alkenes
Koh, Ming Joo,Lee, Boon Chong,Li, Ping,Zhang, Xiaoxiang
supporting information, (2021/12/29)
We present a base-mediated hydroaminatio...
Polymer, and mixture or formulation, and organic electronic device containing same, and monomer thereof
-
Page/Page column 62; 63, (2020/11/23)
Disclosed are a polymer, and a mixture o...
Method for synthesizing N-vinylcarbazole
-
Paragraph 0014-0019, (2019/11/13)
The invention provides a novel method fo...
1484-13-5 Process route
-
-
86-74-8,105184-46-1,97960-57-1
9H-carbazole
-
-
74-86-2,25067-58-7
acetylene
-
-
1484-13-5,25067-59-8
9-vinyl-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
tributylphosphine;
In
N,N-dimethyl acetamide;
at 140 ℃;
for 16h;
under 1.5 Torr;
Glovebox;
Sealed tube;
Autoclave;
|
95% |
|
In
5,5-dimethyl-1,3-cyclohexadiene;
at 140 ℃;
for 9h;
Reagent/catalyst;
Temperature;
|
90% |
|
With
sodium hydroxide; cyclohexane; zinc(II) oxide;
at 145 ℃;
|
|
|
With
1-methyl-pyrrolidin-2-one; potassium hydroxide;
at 150 ℃;
|
|
|
With
soda lime;
at 320 ℃;
|
|
|
With
potassium hydroxide; cyclohexane; zinc(II) oxide; zinc;
at 180 ℃;
|
|
|
With
potassium hydroxide; decalin;
at 170 ℃;
|
|
|
With
sodium hydroxide; cyclohexane; zinc(II) oxide;
at 145 ℃;
|
|
|
With
soda lime;
at 270 ℃;
under 20 Torr;
|
-
-
4901-29-5
9-(1-acetoxyethyl)carbazole
-
-
1484-13-5,25067-59-8
9-vinyl-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
1-methyl-pyrrolidin-2-one;
at 120 - 140 ℃;
for 2.5h;
Temperature;
Reagent/catalyst;
|
81% |
|
With
diisopropylamine;
In
chlorobenzene;
at 120 - 140 ℃;
for 4h;
Reagent/catalyst;
Solvent;
Temperature;
|
80% |
|
With
sodium carbonate;
at 140 ℃;
for 5h;
under 760.051 Torr;
Reagent/catalyst;
Pressure;
Pyrolysis;
|
76% |
1484-13-5 Upstream products
-
1484-14-6
2-carbazol-9-yl-ethanol
-
75-01-4
chloroethylene
-
33650-07-6
potassium carbazole
-
86-74-8
9H-carbazole
1484-13-5 Downstream products
-
114380-50-6
9-(2-p-tolylmercapto-ethyl)-carbazole
-
86-28-2
N-ethylcarbazole
-
101212-70-8
4-benzoyl-6-carbazol-9-yl-2-phenyl-5,6-dihydro-4H-[1,3,4]oxadiazine
-
31317-52-9
9-(3,4,4-tricyano-1,3-butadienyl)carbazole
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-
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