120-70-7
- Product Name：N,N'-Bis(salicylidene)-1,3-propanediamine
- Molecular Formula：C17H18 N2 O2
- Purity：99%
- Molecular Weight：282.342
Product Details;
CasNo： 120-70-7
Molecular Formula： C17H18 N2 O2
factory and supplier 120-70-7 N,N'-Bis(salicylidene)-1,3-propanediamine in stock
- Molecular Formula:C17H18 N2 O2
- Molecular Weight:282.342
- Melting Point:51-53°C
- Boiling Point:510.1°Cat760mmHg
- PKA:12.55±0.50(Predicted)
- Flash Point:191.7°C
- PSA：65.18000
- Density:1.288g/cm3
- LogP:3.02590
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120-70-7 Process route
-
-
90-02-8
salicylaldehyde
-
-
109-76-2,54018-94-9
Trimethylenediamine
-
-
120-70-7
N,N'-propane-1,3-diylbis(salicylideneimine)
| Conditions | Yield |
|---|---|
|
In
ethanol;
at 20 ℃;
for 4h;
Reflux;
|
100% |
|
In
methanol;
at 20 ℃;
for 0.5h;
|
97% |
|
In
ethanol;
|
97% |
|
In
ethanol;
Heating;
|
95% |
|
In
ethanol;
Heating;
|
95% |
|
In
ethanol;
Reflux;
|
95% |
|
In
ethanol;
Heating;
|
95% |
|
In
ethanol;
Heating;
|
95% |
|
In
methanol;
|
87% |
|
In
methanol;
Reflux;
|
87% |
|
With
acetic acid;
In
ethanol;
Reflux;
|
86% |
|
In
ethanol;
for 5h;
Heating;
|
85% |
|
In
water;
at 20 ℃;
for 2h;
|
84% |
|
In
benzene;
for 6h;
Heating;
|
80% |
|
In
methanol;
for 2h;
|
79.69% |
|
In
ethanol;
for 1h;
Reflux;
|
72% |
|
In
ethanol;
at 70 - 80 ℃;
for 4h;
|
71% |
|
In
methanol;
at 50 ℃;
for 3h;
|
70% |
|
In
ethanol;
|
70% |
|
In
ethanol;
|
|
|
In
ethanol;
for 0.5h;
Heating;
|
|
|
In
ethanol;
for 1h;
Heating;
|
|
|
|
|
|
In
methanol;
for 1h;
Heating;
|
|
|
In
ethanol;
for 2.5h;
Heating;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
ethanol;
Reflux;
|
|
|
In
ethanol;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1.5h;
Reflux;
|
|
|
In
methanol;
for 0.4h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
ethanol;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1.5h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1h;
Reflux;
|
|
|
In
methanol;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1.5h;
Reflux;
|
|
|
In
ethanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 2h;
Solvent;
Reflux;
|
|
|
In
ethanol;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
Alkaline conditions;
|
|
|
In
methanol;
Inert atmosphere;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1.5h;
Reflux;
|
|
|
In
methanol;
for 1.5h;
Reflux;
|
|
|
In
methanol;
for 1h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
methanol;
for 1h;
Reflux;
|
|
|
In
ethanol;
at 80 ℃;
for 12h;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
ethanol;
Reflux;
Inert atmosphere;
Schlenk technique;
|
|
|
In
ethanol;
|
|
|
In
ethanol;
for 12h;
Reflux;
|
|
|
In
ethanol;
at 60 ℃;
for 0.5h;
|
|
|
In
methanol;
for 2h;
Reflux;
|
|
|
In
ethanol;
Heating;
|
|
|
In
methanol;
|
|
|
In
ethanol;
at 20 ℃;
for 0.5h;
|
-
-
90-01-7
salicylic alcohol
-
-
109-76-2,54018-94-9
Trimethylenediamine
-
-
120-70-7
N,N'-propane-1,3-diylbis(salicylideneimine)
| Conditions | Yield |
|---|---|
|
salicylic alcohol;
With
dihydrogen peroxide;
at 20 ℃;
for 0.166667h;
Green chemistry;
Trimethylenediamine;
for 5.5h;
Catalytic behavior;
Green chemistry;
|
90% |
|
Trimethylenediamine;
In
ethanol;
at 20 ℃;
Green chemistry;
salicylic alcohol;
With
oxygen;
In
ethanol;
for 1.38333h;
under 760.051 Torr;
Catalytic behavior;
Reflux;
Green chemistry;
|
88% |
120-70-7 Upstream products
-
90-02-8
salicylaldehyde
-
109-76-2
Trimethylenediamine
-
89-95-2
2-methyl-benzyl alcohol
-
118-93-4
o-hydroxyacetophenone
120-70-7 Downstream products
-
74633-23-1
17-phenyl-8,9-dihydro-7H-16,18-dioxa-6,10-diaza-17-bora-dibenzo[a,f]cyclotetradecene
-
2287-28-7
N,N'-bis(2-hydroxybenzyl)-1,3-diaminopropane
-
126796-69-8
{Mn(saltm)SO2}
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