37500-95-1
- Product Name：3,6-Di terbutyl carbazole
- Molecular Formula：C20H25 N
- Purity：99%
- Molecular Weight：279.425
Product Details;
CasNo： 37500-95-1
Molecular Formula： C20H25 N
factory and supplier 37500-95-1 3,6-Di terbutyl carbazole in stock
- Molecular Formula:C20H25 N
- Molecular Weight:279.425
- Melting Point:233-235℃
- Boiling Point:424.2±14.0 °C(Predicted)
- PKA:17.70±0.30(Predicted)
- PSA：15.79000
- Density:1.037
- LogP:5.91610
37500-95-1 Relevant articles
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Two highly emissive carbazole-containing...
37500-95-1 Process route
-
-
507-20-0
tertiary butyl chloride
-
-
86-74-8,105184-46-1,97960-57-1
9H-carbazole
-
-
37500-95-1
3,6-di(tert-butyl)-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 8h;
|
95% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
|
94% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
Sonication;
|
92% |
|
With
zinc(II) chloride;
In
nitromethane;
for 16h;
Inert atmosphere;
|
86% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
|
85% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
|
85% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
|
85% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 24h;
|
83% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 6h;
Inert atmosphere;
|
81% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
|
81% |
|
With
aluminum (III) chloride;
In
nitromethane;
at 20 ℃;
Inert atmosphere;
Schlenk technique;
|
79% |
|
With
zinc(II) chloride;
Inert atmosphere;
|
77% |
|
In
nitromethane;
at 20 ℃;
for 8h;
Inert atmosphere;
|
76% |
|
With
nitromethane; zinc(II) chloride;
for 15.33h;
Glovebox;
Inert atmosphere;
|
75% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 25 ℃;
for 24h;
|
75% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
|
73% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 12h;
Inert atmosphere;
Schlenk technique;
|
70% |
|
With
zinc(II) chloride;
In
nitromethane;
Inert atmosphere;
|
70% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
|
69% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 16h;
Inert atmosphere;
|
66% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 10h;
|
65% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
|
61% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
|
60.6% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 10.3333h;
Cooling with ice;
|
60% |
|
9H-carbazole;
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 0.166667h;
tertiary butyl chloride;
In
nitromethane;
for 5h;
|
55% |
|
With
aluminium trichloride;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
|
54% |
|
With
aluminum (III) chloride;
at 20 ℃;
for 24h;
|
54% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
|
54% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 9h;
|
54% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
|
54% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
|
54% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
|
51% |
|
With
aluminum (III) chloride;
|
50% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 6h;
Inert atmosphere;
|
50% |
|
With
aluminium trichloride;
In
dichloromethane;
at 20 ℃;
for 16h;
|
47% |
|
With
zinc(II) chloride;
In
nitromethane;
Inert atmosphere;
|
46% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 24h;
Inert atmosphere;
|
45% |
|
With
aluminum (III) chloride;
In
chloroform;
at 0 ℃;
for 12h;
|
40% |
|
9H-carbazole;
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
Inert atmosphere;
tertiary butyl chloride;
In
nitromethane;
at 20 ℃;
for 5h;
|
40% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
|
39% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 48h;
|
37.4% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 168h;
Inert atmosphere;
|
36% |
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
35% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 20.5h;
|
32% |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 20.5h;
Inert atmosphere;
|
32% |
|
With
zinc(II) chloride;
In
nitromethane;
for 5h;
|
11% |
|
With
zinc(II) chloride;
In
nitromethane;
for 5h;
|
11% |
|
With
aluminium trichloride;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 40 - 50 ℃;
for 5h;
|
|
|
With
aluminium trichloride;
|
|
|
With
aluminium trichloride;
In
dichloromethane;
|
|
|
With
aluminium trichloride;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 40 - 50 ℃;
|
|
|
With
aluminum (III) chloride;
at 20 ℃;
for 24h;
|
|
|
With
zinc(II) chloride;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
Molecular sieve;
Inert atmosphere;
|
64.5 mg |
|
With
N-Bromosuccinimide;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
Inert atmosphere;
Schlenk technique;
|
|
|
With
aluminum (III) chloride;
Inert atmosphere;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
|
|
|
With
aluminum (III) chloride;
|
|
|
With
aluminum (III) chloride;
In
nitromethane;
at 20 ℃;
for 24h;
|
|
|
With
nitromethane; zinc(II) chloride;
at 20 ℃;
for 5h;
Inert atmosphere;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
Inert atmosphere;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 24h;
|
|
|
With
aluminum (III) chloride;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 5h;
|
|
|
With
aluminum (III) chloride;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 24h;
|
|
|
With
aluminum (III) chloride;
In
chloroform;
for 16h;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
Inert atmosphere;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 ℃;
for 12h;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
|
|
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 24h;
|
|
|
With
aluminum (III) chloride;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
9.6 g |
|
With
zinc(II) chloride;
In
nitromethane;
at 20 ℃;
for 24h;
|
|
|
With
zinc(II) chloride;
In
nitromethane; dichloromethane;
for 0.5h;
Sonication;
|
-
-
2,2'-bis(acetamido)-5,5'-di-tert-butylbiphenyl
-
-
37500-95-1
3,6-di(tert-butyl)-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
phosphoric acid;
In
diethylene glycol;
at 200 ℃;
for 24h;
|
74% |
37500-95-1 Upstream products
-
507-20-0
tertiary butyl chloride
-
86-74-8
9H-carbazole
-
34601-54-2
1,3,6,8-tetra-tert-butyl-9H-carbazole
-
7646-85-7
zinc(II) chloride
37500-95-1 Downstream products
-
320575-24-4
4-(3,6-di-tert-butyl-9H-carbazole-9-yl)benzaldehyde
-
954497-15-5
9,9-bis[4-(3,6-di-tert-butyl-9-carbazolyl)phenyl]fluorene
-
1006377-66-7
1,2-dicyano-trans-1,2-bis(4-(3,6-di(tert-butyl)carbazol-9-yl)phenyl)ethylene
-
1224836-18-3
C66H64N2O2
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-
2,5-Dimethoxy-Beta-NitrostyreneCAS：40276-11-7
-
1,4-Bis(diphenylphosphino)butaneCAS：7688-25-7
-
5-Bromo-2-fluorotolueneCAS：51437-00-4
